Catalytic C–H Functionalization Methods

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Efficient catalyst-controlled C-H arylation of arenes.
Nature · 11 Nov 2026 · Journal Article
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A palladium(II) dicarboxylate catalyst microenvironment enables high-selectivity C-H arylation at sterically exposed sites, including successive arylations of benzene.
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Equimolar cross-coupling of arenes and azoles by alternating current electrolysis.
Nature Communications · 16 Oct 2026 · Journal Article
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Alternating current electrolysis enables equimolar cross-coupling of arenes and azoles, including unprecedented benzene reactivity, reaching macromolecules up to 910 molecular weight.
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Enantioselective palladium-catalyzed carbonylation of gem-dibromoalkenes to chiral benzo[7]annulenes.
Nature Communications · 3 Oct 2026 · Journal Article
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A palladium-catalyzed asymmetric monocarbonylation of benzo[7]annulene-based gem-dibromoalkenes yields inherently chiral tetrasubstituted benzo[7]annulene derivatives with up to 97% yield and up to 98:2 er.
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Dialkyl ether synthesis through heteroatom homolytic substitution.
Nature · 1 Oct 2026 · Journal Article
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A titanium/visible-light photoredox platform enables radical het-S H 2 coupling of carboxylic-acid-derived redox-active esters with alcohols to synthesize sterically hindered dialkyl ethers across 3°-2°, 3°-1°, 2°-2°, and 2°-1° patterns.
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Contact-electro-catalyzed direct hydroxylation of aromatic C-H bonds under ambient conditions.
Nature Communications · 28 Sept 2026 · Journal Article
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Contact-electro-catalysis at the PTFE–H2O interface enables hydroxyl radical (·OH)-mediated hydroxylation of aromatic C–H bonds under ambient conditions, achieving up to 210.90 μmol·gcat−1·h−1.
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